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Laboratory Development
Experimental Set-up (Designed & Fabricated)
Fabricated Equipment
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Several
experimental set-ups with stainless steel UF/RO
cells; stirred batch (450 ml, 600 ml)
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radial cross flow (40 mm dia, 76 mm dia)
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Rectangular thin channel cross flow (6 cm x 40 cm).
A 250 ml stirred reactors of stainless steel
|Multi-component
ED cells|Dialyzer|
Pyrolysis reactor|
Lamella settler|
Mini Pilot Plant, etc.
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RO/UF
spiral wound membrane modules pilot plant with
automatic controls (Designed by Mr. S.P. Mayor (Permionics)
and Dr. P.K. Bhattacharya; Manufacturer: Permionics,
India) │One bench scale set-up (Plate & Frame
module) for RO (courtesy: Hydrarnautics India Ltd.).
Imported Equipment
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Capillary
Condensation porometer vis-à-vis
Gas permeability Tester (PMI-USA): measuring
permeability, pore size, etc.
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RO/UF
experimental set-up with radial cross
flow cell (Berghoff, Germany) |
RO/UF completely equipped experimental
set-up from DSS (Denmark) |
UF batch stirred cells (Chem. Lab., UK
and Schliecher-Schull, Germany)
ED experimental set-up with multicomponent
cells (Berghoff, Germany) |
Several reciprocating high pressure pumps
|Parr
reactor (Parr-USA).
Enzymatic (immobilized)
Membrane batch Reactor (EMR) |
Liquid membrane supported unit for separation through
facilitated transport.
Instruments
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Atomic
Absorption Spectrophotometer (Bucknell, USA)
• High Performence Liquid Chromatography &
Gel Permeation Chromatography (Waters & Shimdtzu)
• Capillary Condensation porometer/
Gas permeability Tester (PMI-USA): measuring permeability, pore size, etc.
• Electrochemical property analyzer (CH Instruments)
• Membrane casting unit (Pune, India)
• Digital Refractometer of 5-decimal accuracy (Atago, Japan)
• DBX-50 digital Refractometer with two decimal accuracy (Atago, Japan)
• UV-spectrophotometer (Perkins Elmer - USA, Hitachi - Japan)
• Gas Chromatographs (Nucon, India) & (AIMIL, India)
• Aqualatic BOD analyzer (Germany)
• Ion-meter (5-Star from Orion & ISTEK-Korea)
• Water Quality Analyzer (Eutech Instruments, Singapore)
• COD reactor (Hach, USA)
• Colorimeter (Hach, USA)
• Turbidity Meter (Hach, USA)
• Pervaporator (Pervasep,USA)
• Water Testing Analyzer
• Milli – Q water purification unit (Millipore)
• Remi high speed centrifuge
• Refrigerated centrifuge (Thermo-Scientific)
Membranes
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Pervaporation membranes of both hydrophilic and
hydrophobic varieties (Sulzer Chemtech, Germany) │47
mm Dia Micro-porous hydrophobic membranes (Millipore
& Pall India) │ Cellulose acetate membranes of 76 mm
dia. of various cut-off sizes (Spectrum, USA; Chem.
Lab, UK) │Flat sheet membranes of different
polymeric base including ion-exchange membranes
(courtesy: Permionics, India; Hydranautics, India;
Millipore, UK; Ashahi, Japan; DSS, Denmark, etc.), Nafion® membranes (DuPont, USA).
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